HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-chloro-N-(5-cyano-2-methylphenyl)acetamide → cis-2-[4-(3-Cyanobenzenesulphonyl)-3,5-dimethylpiperazin-1-yl]-n-(5-cyano-2-methylphenyl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-chloro-N-(5-cyano-2-methylphenyl)acetamide | HCID 22273411 | — |
| Reactant | cis-1-(3-Cyanobenzenesulphonyl)-2,6-dimethylpiperazine | HCID 69744750 | — |
| Product | cis-2-[4-(3-Cyanobenzenesulphonyl)-3,5-dimethylpiperazin-1-yl]-n-(5-cyano-2-methylphenyl)acetamide | HCID 69745774 | — |
Reaction Steps
The title compound was prepared from the product of step (i) (0.19 g) and the product from Example 80 step (ii) (0.2 g) by the method of Example 80 step (iii) as a white solid. Yield: 0.25 g
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06969713B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-e70d5c1c298e4bc79df3685c4756b6e0 |
| Source note | uspto-grants-2005_11 |