Tetrafluoro-m-phenylenediamine dihydrochloride → HCID 22272755, compound

Participants

Reaction Steps

After that, the same reaction and treatment as in Example 24 were conducted using N-[2,4-bis(isopropylthio)-6-methyl-3-pyridyl]-2-bromoacetamide instead of N-[2,4-bis-(methylthio)-6-methyl-3-pyridyl]-2-bromoacetamide and the resulting 2-[4-[2-(benzoxazol-2-ylthio)-ethyl]piperazin-1-yl]-N-[2,4bis(isopropylthio)-6-methyl-3-pyridyl]acetamide was converted to a dihydrochloride to provide a desired compound as colorless powdery crystals.

Provenance & Evidence