HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorine → HCID 20541100, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | Methyl 3-iodobenzoate | HCID 69258 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 20541100 | HCID 20541100 | — |
Reaction Steps
A solution of 5.0 g methyl-m-iodobenzoate in 70 ml chloroform was cooled to 0°-10° and treated with gaseous chlorine for 1 hour. The resulting yellow solution was evaporated to afford 6.2 g methyl-m-iodobenzoate dichloride as yellow needles, mp=108°-110°. IR: 5.83, 7.80, 8.00, 8.90, 9.18, 10.52, 11.12, 12.39, and 13.48.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04328162 |
| Source dataset | uspto-grants-1982_05 |
| ORD ID | ord-430ff9281a904a6f9c93127fe7a25470 |
| Source note | uspto-grants-1982_05 |