HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12850270, compound → HCID 53843008, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12850270 | HCID 12850270 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53843008 | HCID 53843008 | — |
Reaction Steps
A mixture of 12.4 g of 2-(methylmercaptoacetylamino)-4-[(2-methylpropyl)thio]nitrobenzene, 1.3 g PtO2 and 200 ml of ethanol is reduced on the Parr hydrogenator at 50 psi until the required amount of H2 is absorbed. The mixture is filtered, the solvent removed and the residue used immediately in the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04328241 |
| Source dataset | uspto-grants-1982_05 |
| ORD ID | ord-25b5c6b30d7149059f4a166f43397aac |
| Source note | uspto-grants-1982_05 |