HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → HCID 20499880, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | 2,3,4,5,6,7,8,9,10,11,12,13-Dodecahydro-2-methyl-1H-cyclopentacyclododecene | HCID 14609946 | — |
| Product | HCID 20499880 | HCID 20499880 | 92% |
Reaction Steps
Pure 14-methyl-bicyclo[10.3.0]pentadec-1(12)-ene (C) was also prepared as follows: 0.53 g of the above 10:1 mixture of compounds C and D were heated during 4 h 1/2 in the presence of 0.02 g of iodine, under argon atmosphere. After distillation of the reaction mixture (b.p. 100°-110° /0.01 Torr) there were isolated 0.48 g (92% yield) of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04328383 |
| Source dataset | uspto-grants-1982_05 |
| ORD ID | ord-bc510d47cfb44311a608ed63275d8afb |
| Source note | uspto-grants-1982_05 |