Acetone → HCID 12906590, compound

Participants

Reaction Steps

In acetone (40 ml) was dissolved N-(2-fluoro-4-chlorophenyl)-3,4,5,6-tetrahydroisophthalimide (2.8 g) and while stirring at room temperature, isopropylamine (0.6 g) was added. The mixture was allowed to stand for 10 hours, after which time the precipitate was recovered by filtration and washed with acetone. Yield 3.0 g.; m.p. 188°-189° C.

Provenance & Evidence