Potassium hexafluoroantimonate(1-) → Diphenyliodonium hexafluoroantimonate

Participants

Reaction Conditions

Reaction Steps

A mixture of 4 parts of diphenyliodonium perchlorate and 2.8 parts of potassium hexafluoroantimonate and 100 parts of methanol was stirred for 1 hour at 25° C. The resulting mixture was then filtered and the methanol solution evaporated to produce a solid having a melting point of 77°-87° C. Based on method of preparation there was obtained an 86.1% yield of diphenyliodonium hexafluoroantimonate.

Provenance & Evidence