Benzyl Chloride → HCID 54109068, compound

Participants

Reaction Steps

A solution of 2.5 gm of 6-(4-mercapto-butoxy)-3,4-dihydro-carbostyril in 25 ml of dimethysulfoxide was mixed whilst stirring with 1.4 gm of potassium carbonate and subsequently with 1.3 ml of benzyl chloride. After stirring for 15 hours at room temperature, the reaction mixture was diluted with 200 ml of water, and the precipitated oily substance was separated and recrystallized from ethyl acetate.

Provenance & Evidence