Hydrogen Peroxide → HCID 20539972, compound

HRID 1065396Notes

Reaction equation

[C:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[S:10][CH2:11][CH2:12][CH2:13][CH2:14][O:15][C:16]1[CH:17]=[C:18]2[C:23](=[CH:24][CH:25]=1)[NH:22][C:21](=[O:26])[CH2:20][CH2:19]2)([OH:3])=[O:2].[OH:27]O>>[C:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[S:10]([CH2:11][CH2:12][CH2:13][CH2:14][O:15][C:16]1[CH:17]=[C:18]2[C:23](=[CH:24][CH:25]=1)[NH:22][C:21](=[O:26])[CH2:20][CH2:19]2)=[O:27])([OH:3])=[O:2]

Participants

Reactant 2

HCID 784Hydrogen Peroxide

HCID 20539994HCID 20539994, compound

Product 1

HCID 20539972HCID 20539972, compoundYield 77.2%

Procedure

Prepared analogous to Example 123 from 6-[4-(2-carboxyphenyl-mercapto)-butoxy]-3,4-dihydro-carbostyril and hydrogen peroxide. M.p.: 194°-196° C. Yield: 77.2% of theory.

Sources & evidence

ORD record: ord-95d9436f54bc43d99ee792a2c92bd7fb
Source dataset: uspto-grants-1982_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04329347

Reaction notes

Loading…