Nitroethane → HCID 53769258, compound

HRID 1065469Notes

Reaction equation

HRID 1065469 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][C:9]=1[O:10][CH3:11])[CH:5]=O.C([O-])(=O)C.[NH4+].[N+:17]([CH2:20][CH3:21])([O-:19])=[O:18]>>[CH3:1][C:2]1[CH:3]=[C:4]([CH:5]=[C:20]([N+:17]([O-:19])=[O:18])[CH3:21])[CH:7]=[CH:8][C:9]=1[O:10][CH3:11]

Participants

4

Reactant 3

HCID 6587NitroethaneHCID 1229363-Methyl-4-anisaldehydeHCID 517165Ammonium Acetate

Product 1

HCID 53769258HCID 53769258, compound

Procedure

The starting material is prepared as follows: The mixture of 100 g of 3-methyl-4-methoxybenzaldehyde, 300 ml of nitroethane and 52 g of ammonium acetate is refluxed for 4 hours and evaporated, to yield the 1-(3-methyl-4-methoxyphenyl)-2-nitropropene.

Workup

  1. customThe starting material is prepared
  2. temperatureis refluxed for 4 hours
  3. customevaporated

Sources & evidence

ORD record
ord-5e5670977edd42879f4ce919fe8b3344
Source dataset
uspto-grants-1982_05
Patent number
US04329367

Reaction notes

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