HuagongsheHuagongshe Chemistry Print Report · For research reference only
alpha-Methylene-4-methoxybenzenepropanoic acid → 3-Benzoylthio-2-(p-methoxybenzyl)propionic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | alpha-Methylene-4-methoxybenzenepropanoic acid | HCID 13817412 | — |
| Reactant | HCID 178526132 | HCID 178526132 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 3-Benzoylthio-2-(p-methoxybenzyl)propionic Acid | HCID 12962727 | — |
Reaction Steps
By the method of Preparation 7, 2-(p-methoxybenzyl)acrylic acid (3.84 gm., 20 mmoles) was reacted with thiobenzoic acid to yield the title product in essentially quantitative yield [6.61 gm.; Rf 0.48 (ether)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04329495 |
| Source dataset | uspto-grants-1982_05 |
| ORD ID | ord-252fc641da624757ac37407aea11f72a |
| Source note | uspto-grants-1982_05 |