HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 131712720, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 5-Phenyl-1,3-oxazol-2-ol | HCID 12306996 | — |
| Reactant | HCID 13991420 | HCID 13991420 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 131712720 | HCID 131712720 | — |
Reaction Steps
16.1 g (0.1 mol) of 5-phenyl-4-oxazolin-2-one are dissolved in 100 ml of absolute DMF and 25.6 g (0.12 mol) of ethoxycarbonylheptyl isocyanate are added. The mixture is stirred for 24 hours at 50°-60° C., water is added and the oily/crystalline precipitate which is formed is separated, washed with water and dried in vacuo at room temperature. The crude product is recrystallised from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04330550 |
| Source dataset | uspto-grants-1982_05 |
| ORD ID | ord-02add52faab644d886d1a7657315e72b |
| Source note | uspto-grants-1982_05 |