HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 20539740, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 53863676 | HCID 53863676 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20539740 | HCID 20539740 | — |
Reaction Steps
A solution of 1.6 g N-(7-methyl-3-oxo-1-propyl-4-indanyl)oxamic acid ethyl ester in 100 ml methanol is heated at reflux with 5.28 ml of 1 M aqueous NaOH for 30 minutes. The solution is concentrated, diluted with water, filtered through a filtering aid such as Hyflo (Registered Trade Mark), and made acid with 2 N HCL. The title compound is filtered off and dried. M.Pt. 157°-158°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04330555 |
| Source dataset | uspto-grants-1982_05 |
| ORD ID | ord-c022c94bab7342eeac70a3671c3f5fa2 |
| Source note | uspto-grants-1982_05 |