HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 12961958, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 12961961 | HCID 12961961 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12961958 | HCID 12961958 | 80.5% |
Reaction Steps
Hydrolysis of 17α-amino-5α-androstane-3β,16α-diol 3-acetate (4.8 g) with sodium hydroxide (4 N) and ethanol at reflux temperature gave 17α-amino-5α-androstane-3β,16α-diol (3.4 g). Crystallisation from ethanol yielded an analytical sample, m.p. 220°-225° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04330539 |
| Source dataset | uspto-grants-1982_05 |
| ORD ID | ord-b21bd65b87bb48ad8a6311e48df10149 |
| Source note | uspto-grants-1982_05 |