Water → HCID 12850209, compound

Participants

Reaction Steps

Nine and four tenths grams (9.4 g) of 2-(m-aminophenyl)-5,5-diethyl-1,3-dioxane was reacted with 3 g of methyl isocyanate in 75 ml of acetone. The mixture was refluxed for between one and two hours and poured into water and the product collected by filtration. The yield was 11.7 g of the title compound, m.p. 112°-125° C. Trituration with diethyl ether raised the melting point to 135°-137° C.

Provenance & Evidence