HRID1065948

反应详情

EQUATION

反应方程式

HRID 1065948 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

The hydrogen reduction of this 3-octyn-1-ol is carried out by dissolving the compound in n-hexane with addition of 3 to 20% by weight of a Lindlar catalyst and introducing hydrogen at room temperature with agitation (reaction (iii)). Removal of the catalyst by filtration and n-hexane by distillation from the reaction mixture gives cis-3-octen-1-ol in an almost quantitative yield.

WORKUP

后处理

  1. customRemoval of the catalyst
  2. filtrationby filtration and n-hexane
  3. distillationby distillation from the reaction mixture