HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Octyn-1-ol → 3-Octen-1-ol, (3Z)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Octyn-1-ol | HCID 84694 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Lindlars catalyst | HCID 131709914 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | 3-Octen-1-ol, (3Z)- | HCID 5364519 | — |
Reaction Steps
The hydrogen reduction of this 3-octyn-1-ol is carried out by dissolving the compound in n-hexane with addition of 3 to 20% by weight of a Lindlar catalyst and introducing hydrogen at room temperature with agitation (reaction (iii)). Removal of the catalyst by filtration and n-hexane by distillation from the reaction mixture gives cis-3-octen-1-ol in an almost quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04331820 |
| Source dataset | uspto-grants-1982_05 |
| ORD ID | ord-a2c654ff179d4d5aa4d1b5b7c0059193 |
| Source note | uspto-grants-1982_05 |