HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → HCID 178456961, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | Isopropyl Isothiocyanate | HCID 75263 | — |
| Reactant | HCID 21197855 | HCID 21197855 | — |
| Reactant | HCID 21197876 | HCID 21197876 | — |
| Product | HCID 178456961 | HCID 178456961 | — |
Reaction Steps
Starting from 2-amino-5-tert-butylbenzenesulfonamide and isopropyl isothiocyanate, and following a procedure analogous to the one described in Example 4a, N-(2-amino-5-tert-butylbenzenesulfonyl)-N′-isopropylthiourea was prepared; m.p. 128-130° C. Subsequent ring closure with phosgene by a procedure analogous to the one described in Example 4b gave the title compound; m.p. 290-293° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06242443B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-cca17fe217d34107be4107b1c7e02978 |
| Source note | uspto-grants-2001_06 |