3,3-Diphenylpropylamine → HCID 178527190, compound

Participants

Reaction Steps

Starting from 3,7-dichloro-4H-1,2,4-benzothiadiazine 1,1-dioxide (300 mg; 1.19 mmol) and 3,3-diphenylpropylamine (1.5 g; 7.1 mmol) with the use of same procedure as in example 21 300 mg (59%) of the title compound was prepared; 1H-NMR (DMSO-d6) ppm; 10.7 (s, 1H, NH), 7.68 (d, 1H, H-8), 7.60 (dd, 1H, H-5), 7.25 (m, 11H, ), 4.1 (t, 1H, CH), 3.11 (q, 2H, CH2), 2.35 (q, 2H, CH2); MS:EI/70eV: 425 (M+), 245, 193, 180, 165, 152, 115.

Provenance & Evidence