Benzenebutanamine → HCID 178527191, compound

Participants

Reaction Steps

Starting from 3,7-dichloro-4H-1,2,4-benzothiadiazine 1,1-dioxide (300 mg; 1.19 mmol) and 4-phenylbutylamine (1.5 g; 4.12 mmol) and with the use of same procedure as in example 21 120 mg (27.7%) of the title compound was prepared.; 1H-NMR (DMSO-d6) ppm; 10.8 (s, 1H, NH), 7.75 (d, 1H, H-8), 7.60 (dd, 1H, H-5), 7.2 (m, 7H), 3.29 (t, 2H, CH2), 2.66 (t, 2H, CH2), 1.5 (m, 4H, 2×CH2); MS:EI/70eV: 363 (M+), 272, 259, 231, 180, 91, 44.

Provenance & Evidence