Isopropyl Isothiocyanate → HCID 178456983, compound

Participants

Reaction Steps

The title compound was prepared from 2-amino-5-iodobenzenesulfonamide and isopropyl isothiocyanate by a method analogous to the one described in Example 4; m.p. 305-307° C. dec; 1H-NMR (DMSO-d6): δ 1.17 (d, 6H, CH(CH3)2), 3.91 (m, 1H, CH(CH3)2), 7.02 (d, 1H, ArH), 7.15 (br., 1H, NH), 7.8-7.9 (m, 2H, ArH), 10.43 (br.s, 1H, NH); MS: m/e 365 (M+, 27%); (C10H12N3I1O2S1) calc. C, 32.89; H, 3.31; N, 11.51, found C, 32.79; H, 3.41; N, 11.27.

Provenance & Evidence