Isopropyl Isothiocyanate → HCID 178456955, compound

Participants

Reaction Steps

The title compound was prepared from 2-amino-3,5-dibromobenzenesulfonamide and isopropyl isothiocyanate by a method analogous to the one described in Example 4; m.p. 306-311° C. (ethyl acetate); 1H-NMR (DMSO-d6): δ 1.19 (d, 6H, CH(CH3)2), 3.90 (m, 1H, CH(CH3)2), 7.82 (d, 1H, ArH), 7.92 (br.d, 1H, NH), 8.16 (d, 1H, ArH), 9.65 (br.s, 1H, NH); MS: m/e 395/397/399 (M+); (C10H11N3Br2O2S1) calc. C, 30.25; H, 2.79; N, 10.58; found C, 30.34; H, 2.77; N, 10.48.

Provenance & Evidence