Allyl Isothiocyanate → HCID 178456967, compound

Participants

Reaction Steps

The title compound was prepared from 2-amino-4-chlorobenzenesulfonamide and allyl isothiocyanate by a method analogous to the one described in Example 4; m.p. 284-286° C. (ethyl acetate); 1H-NMR (DMSO-d6): δ 3.88 (distorted t, 2H, NHCH2), 5.1-5.3 (m, 2H, ═CH2), 5.78-6.0 (m, 1H, ═CH), 7.22-7.35 (m, 2H, ArH), 7.50 (br.t, 1H, NH), 7.69 (d, 1H, ArH), 10.73 (br.s, 1H, NH); MS: m/e 271/273 (M+); (C10H10N3Cl1O2S1) calc. C, 44.20; H, 3.71 N, 15.46; found C, 44.10; H, 3.79; N, 15.32.

Provenance & Evidence