Cyclobutylamine → HCID 178527173, compound

HRID 1066153Notes

Reaction equation

HRID 1066153 reaction equation
O.[Cl:2][C:3]1[C:4]([Cl:20])=[CH:5][C:6]2[S:11](=[O:13])(=[O:12])[N:10]=[C:9]([N:14]3[CH:18]=[CH:17]N=C3)[NH:8][C:7]=2[CH:19]=1.[CH:21]1(N)CC[CH2:22]1>>[CH:18]1([NH:14][C:9]2[NH:8][C:7]3[CH:19]=[C:3]([Cl:2])[C:4]([Cl:20])=[CH:5][C:6]=3[S:11](=[O:12])(=[O:13])[N:10]=2)[CH2:17][CH2:22][CH2:21]1

Participants

3

Reactant 2

HCID 75645CyclobutylamineHCID 21197737HCID 21197737, compound

Product 1

HCID 178527173HCID 178527173, compound

Procedure

6,7-Dichloro-3-(imidazol-1-yl)-4H-1,2,4-benzothiadiazine 1,1-dioxide monohydrate was treated with cyclobutylamine according to the general procedure Method D to give the title compound; m.p. 320-326° C.; IR (KBr): 3290, 3163, 3068, 2979, 2952, 1631, 1580, 1556, 1460, 1331, 1251, 1166, 1152, 1137, 1128 cm−1.

Sources & evidence

ORD record
ord-c203914b3fb1435d8594bb8c6a6d09f6
Source dataset
uspto-grants-2001_06
Patent number
US06242443B1

Reaction notes

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