Bromoacetic Acid → HCID 57163070, compound

HRID 1066246Notes

Reaction equation

[N+:1]([C:4]1[CH:5]=[C:6]2[C:10](=[CH:11][CH:12]=1)[NH:9][CH:8]=[CH:7]2)([O-:3])=[O:2].Br[CH2:14][C:15]([OH:17])=[O:16]>>[N+:1]([C:4]1[CH:5]=[C:6]2[C:10](=[CH:11][CH:12]=1)[N:9]([CH2:14][C:15]([O:17][C:6]([CH3:10])([CH3:7])[CH3:5])=[O:16])[CH:8]=[CH:7]2)([O-:3])=[O:2]

Participants

Reactant 2

HCID 6227Bromoacetic Acid

HCID 225235-Nitroindole

Product 1

HCID 57163070HCID 57163070, compound

Procedure

Prepared according to the method of Example 15a) from 5-nitroindole (0.207 g) and 2-bromoaceticacid, 1,1 -diemthylethyl ester (0.23 ml) to leave sub-title compound as a yellow oily solid (0.29 g).

Workup

customPrepared

Sources & evidence

ORD record: ord-f83b0c0a99ae475a92a066172745400e
Source dataset: uspto-grants-2001_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06242470B1

Reaction notes

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