HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Amino-2-methylphenyl)methanol → HCID 20660019, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Amino-2-methylphenyl)methanol | HCID 577175 | — |
| Reactant | 1-Adamantaneacetyl chloride | HCID 2771882 | — |
| Product | HCID 20660019 | HCID 20660019 | 27.1% |
Reaction Steps
Prepared according to the method of Example 1b) from 1-adamantaneacetyl chloride (2.0 g) and 3-amino-2-methylbenzyl alcohol (1.29 g). Silica gel chromatography, eluting with 5% ethylacetate in dichloromethane gave the title compound as a white solid (0.80 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06242470B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-f99f61b3cc4c4c12945881e5c0713b14 |
| Source note | uspto-grants-2001_06 |