HCID 54012795, compound → HCID 620856, compound

HRID 1066351Notes

Reaction equation

HRID 1066351 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]2[C:13](=[CH:14][CH:15]=1)[C:12]([CH:16](C(OCC)=O)C(OCC)=O)=[C:11]1[C:6]([CH:7]=[CH:8][C:9]([O:27][CH3:28])=[CH:10]1)=[N:5]2>O.Cl>[Cl:1][C:2]1[CH:3]=[C:4]2[C:13](=[CH:14][CH:15]=1)[C:12]([CH3:16])=[C:11]1[C:6]([CH:7]=[CH:8][C:9]([O:27][CH3:28])=[CH:10]1)=[N:5]2

Participants

4

Reactant 1

HCID 54012795HCID 54012795, compound

Product 1

HCID 620856HCID 620856, compound

Reagents, catalysts & solvents 2

HCID 313Hydrochloric AcidSolventHCID 962WaterSolvent

Procedure

A solution of the compound of Example 19 (a) (2.2 g, 5.5 mmol) in water (5 mL) and concentrated hydrochloric acid was heated to reflux for 4 h and filtered to give the title compound. MS(ES) m/e 258.2 (M+H)+.

Workup

  1. temperatureto reflux for 4 h
  2. filtrationfiltered

Sources & evidence

ORD record
ord-c58f70ac2463404ebb619c8f343b931c
Source dataset
uspto-grants-2001_06
Patent number
US06242459B1

Reaction notes

Loading…