HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → Thiophene-2-sulfonyl isocyanate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 2-Thiophenesulfonylamide | HCID 86585375 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | Thiophene-2-sulfonyl isocyanate | HCID 12875192 | — |
Reaction Steps
A mixture of 2-thiophenesulfonylamide (1.5 g) and oxalyl chloride (6 mL) in 10 mL of 1,2-dichloroethane was refluxed for 14 h. The solvent was removed under vacuum and the crude used as is for the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06242493B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-c87843ceab0f4afe83f985e1c0d6e408 |
| Source note | uspto-grants-2001_06 |