HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 21198682, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | 2-Naphthoyl chloride | HCID 75246 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | 3-Bromo-2-methylphenol | HCID 11171430 | — |
| Product | HCID 21198682 | HCID 21198682 | 47% |
Reaction Steps
AlCl3 (17.48 g; 131.1 mmol) was added portionwise to a mixture of 3-bromocresol (16.04 g; 87.4 mmol) and 2-naphthoyl chloride (25.00 g; 131.1 mmol) in 50 mL of CHCl3 gave 14.0 g (47%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06242493B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-fb5ca6969f394e9b94b9f96d7b4d59cf |
| Source note | uspto-grants-2001_06 |