HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1066367Generated: October 30, 2026
Trifluoroacetic acid → HCID 21198710, compound
https://huagongshe.com/reaction/1066367
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Triethylsilane | HCID 12052 | — |
| Reactant | HCID 21198682 | HCID 21198682 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 21198710 | HCID 21198710 | 82% |
Reaction Steps
To the methanone of Step 1 (14.0 g) and triethylsilane (15 mL) in 15 mL of CHCl3 was added TFA and was heated to 50° C. overnight. The solution was cooled and quenched with NaOH (2N) to provide the title compound in 82% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06242493B1 |
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| Source dataset | uspto-grants-2001_06 |
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| ORD ID | ord-f73f2178f3384c61bb5c4b27705a336f |
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| Source note | uspto-grants-2001_06 |
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