Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → Octyl 4'-hydroxy-4-biphenylcarboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | Dichloromethane | HCID 6344 | — |
| 반응물 | Octyl4'-methoxycarbonyloxy-4-biphenylcarboxylate | HCID 18328376 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Octyl 4'-hydroxy-4-biphenylcarboxylate | HCID 14692993 | — |
반응 단계
A solution of compound 5 (5.25 g, 0.014 mol) and aqueous ammonia (35% w/v, 100 ml) in ethanol (200 ml) was stirred for 1 h at room temperature. TLC analysis (dichloromethane) revealed a complete reaction. The solvent was removed in vacuo and the shite solid was recrystallised from ethanol to give colourless crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06242636B1 |
| 출처 데이터셋 | uspto-grants-2001_06 |
| ORD ID | ord-4c0928ed998b44f0abc8a9f40a5bde1b |
| 출처 메모 | uspto-grants-2001_06 |