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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1066565Generated: November 1, 2026

HCID 304320, compound → HCID 45490076, compound

https://huagongshe.com/reaction/1066565

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 304320HCID 304320—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 45490076HCID 4549007699.2%

Reaction Steps

To a solution of 2-(4-methoxybenzylidene)succinic acid 1-methyl ester (3 g) in methanol (100 ml) was added 10% palladium on carbon (0.6 g) and the solution was stirred for 16 hours under hydrogen atomosphere at room temperature. The catalyst was filtered off and the filtrate was concentrated under reduced pressure to give the titled compound (3 g) as a colorless oily substance.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06242600B1
Source datasetuspto-grants-2001_06
ORD IDord-31e0d3b9f2914c0da178ac34b6cce0c9
Source noteuspto-grants-2001_06