HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 304320, compound → HCID 45490076, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 304320 | HCID 304320 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 45490076 | HCID 45490076 | 99.2% |
Reaction Steps
To a solution of 2-(4-methoxybenzylidene)succinic acid 1-methyl ester (3 g) in methanol (100 ml) was added 10% palladium on carbon (0.6 g) and the solution was stirred for 16 hours under hydrogen atomosphere at room temperature. The catalyst was filtered off and the filtrate was concentrated under reduced pressure to give the titled compound (3 g) as a colorless oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06242600B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-31e0d3b9f2914c0da178ac34b6cce0c9 |
| Source note | uspto-grants-2001_06 |