1-Hexanol → Decane

Using the surfactant tridodecylmethylammonium chloride (TDAC) at a concentration of approximately 8%, hexanol at 10%, and the remainder octane, MOS2 particles are formed with an average diameter, as determined by lights-cattering and high-resolution transmission electron microscopy (HRTEM), of approximately 3.0 nm. In a solution using the surfactant didodecyldimethylammonium bromide (DDAB) at a concentration of approximately 10%, hexanol at 11%, and the remainder decane, MoS2 particles are formed with an average diameter, as determined by light-scattering and transmission electron microscopy techniques, of approximately 4.5 nm. In a solution using the surfactant DDAB in toluene at a concentration of approximately 0.5%, MoS2 particles are formed with an average diameter, as determined by light-scattering and TEM, of approximately 8-10 nm. The as-synthesized MOS2 clusters were purified to remove excess reactants, surfactants or reaction by-products by extraction from octane into acetonitrile, dried, and then added to water to form the catalyst solution as noted above.

ORD record

ord-1c31daa3ebfc44cba0e560414a87b1e2

Source dataset

uspto-grants-2001_06

DOI

10.6084/m9.figshare.5104873.v1

Patent number

US06245200B1