HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → HCID 21195990, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | HCID 21196110 | HCID 21196110 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21195990 | HCID 21195990 | — |
Reaction Steps
Under an argon atmosphere 2-[(4-chlorophenoxy)methyl]-1-[2-(1-tritylpiperidin-4-yl)ethyl]-1H-indole was dissolved in 7.0 ml of methylene chloride. The reaction solution was then placed on an ice bath and formic acid (0.3383 g) was added. The resulting mixture was stirred in the ice bath for about five hours. The progress of the reaction was monitored by thin layer chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06245761B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-7a7a1bfa43984058a33bb1fc3be89cb9 |
| Source note | uspto-grants-2001_06 |