HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Piperidinamine, N,N-dimethyl- → HCID 54146532, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Piperidinamine, N,N-dimethyl- | HCID 142690 | — |
| Reactant | 1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride | HCID 2723939 | — |
| Reactant | HCID 54353537 | HCID 54353537 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54146532 | HCID 54146532 | — |
Reaction Steps
Under a nitrogen atmosphere dimethylaminopiperidine was dissolved in 3.0 ml of methylene chloride. To this solution were added 3-(2-[(4-chlorophenoxy)methyl]-1-methyl-1H-indol-3-yl]prop-2-enoic acid (0.050 g, 0.1462 mmol) and 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride (0.0356 g, 0.278 mmol). The resulting mixture was stirred at room temperature overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06245761B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-feba1f9b7c3f4d1cb2bb54f9d488f296 |
| Source note | uspto-grants-2001_06 |