HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 21196068, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 21195973 | HCID 21195973 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21196068 | HCID 21196068 | — |
Reaction Steps
Under a nitrogen atmosphere in a round bottom flask 2-[(4-chlorophenoxy)methyl]-1-methyl-3-[2-(methoxycarbonyl)ethyl]-1H-indole (0.275 g, 0.771 mmol) was dissolved in 8 ml of dry tetrahydrofuran. To this solution was added 4.0 ml of a 2.0 N lithium hydroxide solution. The reaction mixture was stirred at room temperature overnight. The progress of the reaction was monitored by thin layer chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06245761B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-7421cf4781d84dd5b283e5aa5fe10e11 |
| Source note | uspto-grants-2001_06 |