HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Aminophthalide → 5-[4-(4-Bromo-2-methoxyphenyl)-2-oxo-valeroylamino)-phthalide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Aminophthalide | HCID 720669 | — |
| Reactant | 4-(4-Bromo-2-methoxyphenyl)-2-oxo-valeric acid | HCID 18551187 | — |
| Reactant | 4-Bromo-5-(4-methyl-2-oxo-4-phenyl-valeroylamino)-phthalide | HCID 18551202 | — |
| Product | 5-[4-(4-Bromo-2-methoxyphenyl)-2-oxo-valeroylamino)-phthalide | HCID 21196820 | — |
Reaction Steps
was obtained analogously to the process that is described for 4-bromo-5-(4-methyl-2-oxo-4-phenyl-valeroylamino)-phthalide from 5-aminophthalide and 4-(4-bromo-2-methoxyphenyl)-2-oxo-valeric acid, melting point 136-140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06245804B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-7d9bf01768c549cbbaae2c3b5ef93be9 |
| Source note | uspto-grants-2001_06 |