HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Diphenylethylamine → HCID 131722639, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Diphenylethylamine | HCID 77575 | — |
| Reactant | HCID 122173709 | HCID 122173709 | — |
| Product | HCID 131722639 | HCID 131722639 | — |
Reaction Steps
Using Procedure A, Nα-Boc-Nδ-Fmoc-Nα-methylornithine and 2,2-diphenylethylamine afforded a colorless solid: 1H NMR (400 MHz, CDCl3) δ1.39 (s, 10H), 1.57 (m, 2H), 1.77 (m, 1H), 1.98 (m, 1H), 2.50 (s, 3H), 3.19 (m, 2H), 3.80 (m, 1H), 4.00 (m, 1H), 4.19 (t, J=9.5 Hz, 1H), 4.22 (m, 1H), 4.40 (d, J=7.2 Hz, 2H), 4.46 (m, 1H), 7.20-7.34 (m, 12H), 7.41 (t, J=6.6 Hz, 2H), 7.60 (d, J=8.0 Hz, 2H), and 7.79 (d, J=8.5 Hz, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06245746B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-5ebff82fb06c47fba07dc164fec35953 |
| Source note | uspto-grants-2001_06 |