HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54433463, compound → HCID 21196513, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54433463 | HCID 54433463 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21196513 | HCID 21196513 | 89.6% |
Reaction Steps
A mixture of 3-{[3-(4,5-diphenyloxazol-2-yl)bicyclo-[2.2.1]hept-2-en-2-yl]methyl}benzoic acid (0.3 g) and 10% Pd/C (0.1 g) in methanol (20 ml) was stirred under H2 for 8 hours. The catalyst was filtered off and filtrate was evaporated in vacuo to give 3-{[3-(4,5-diphenyloxazol-2-yl)-bicyclo[2.2.1]hept-2-yl]methyl}benzoic acid (0.27 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06245790B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-7d9209b8b14d447e95308f15daf9e07c |
| Source note | uspto-grants-2001_06 |