関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | HCID 178418600 | HCID 178418600 | — |
| 反応物 | HCID 178502822 | HCID 178502822 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178502825 | HCID 178502825 | — |
反応手順
About 582 mg (3.34 mole) of particulate arginine was dissolved in 50 ml of distilled water. Additionally, about 1.0 grams (1.67 mole) of ceftriaxone was dissolved in 50 ml of a separate volume of distilled water. The solution containing arginine was adjusted with 1N-HCl until the pH reached 6.0. The ceftriaxone solution was then added to the arginine solution and stirred by a magnetic stirrer at room temperature for 1 hour forming a ceftriaxone-arginine solution. To the ceftriaxone-arginine solution was added about 400 mg of carrageenan and the solution was stirred by magnetic stirrer at room temperature for 2 hours. A ceftriaxone-arginine-carrageenan complex was formed which was freeze-dried while in the swollen state, yielding about 1.84 g of the freeze dried complex.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US06248360B1 |
|---|
| 出典データセット | uspto-grants-2001_06 |
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| ORD ID | ord-35d26ea3d04d43a59978e30abc855c17 |
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| 出典メモ | uspto-grants-2001_06 |
|---|