Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thiophosgene | HCID 10040 | — |
| Reactant | HCID 14273590 | HCID 14273590 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 21192204 | HCID 21192204 | — |
Reaction Steps
11.5 g (100 mmol) of thiophosgene is added to 22.12 g (100 mmol) of 3-(4-aminophenyl)-glutaric acid in 300 ml chloroform and heated for 50 minutes at 40° C. It is evaporated to dryness and the residue is crystallized from a little isopropanol/ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06248306B1 |
|---|
| Source dataset | uspto-grants-2001_06 |
|---|
| ORD ID | ord-945f31b5a1cf4871baf879ee94d89b94 |
|---|
| Source note | uspto-grants-2001_06 |
|---|
