HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178478796, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178512626 | HCID 178512626 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178478796 | HCID 178478796 | — |
Reaction Steps
1-Guanidino-7-sulphamoylisoquinoline (12 mg, 0.045 mmol) was dissolved in a solution of ethanol saturated with HCl gas (1.0 mL) and the mixture was stirred at room temperature for 1 hour. The solvents were evaporated in vacuo and the residue was azeotroped with dichloromethane (CH2Cl2) to give 1-guanidino-7-sulphamoylisoquinoline dihydrochloride (13 mg, 0.043 mmol) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248738B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-c469418715794444b8aeac6ae95ad142 |
| Source note | uspto-grants-2001_06 |