HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethoxybenzoic acid → 3-BROMO-4-ETHOXYBENZOIC ACID
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethoxybenzoic acid | HCID 12093 | — |
| Reactant | Bromine | HCID 24408 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 3-BROMO-4-ETHOXYBENZOIC ACID | HCID 3116194 | — |
Reaction Steps
To a solution of 4ethoxybenzoic acid (3.6 g, 0.022 mol) in chloroform (60 ml) was added bromine (1.13 ml, 0.022 mol) in chloroform (20 ml) dropwise. After stirring overnight at room temperature the precipitate was filtered off and dried to afford the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248754B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-f98146b56e02444fa978c9f341886fd9 |
| Source note | uspto-grants-2001_06 |