Water → HCID 21192916, compound

Participants

Reaction Steps

N-(8-Chloro-1,2,3,4-tetrahydroisoquinolin-7-yl)-4-methoxy-3-trifluoromethylbenzamide (0.193 g) in dichloromethane (10 ml) containing triethylamine (0.055 ml) was treated with methanesulfonyl chloride ((0.063 g) and the mixture stirred for 48 h. Water was added and the organic phase separated and solvent removed at reduced pressure. The residue was triturated with diethyl ether to give the title compound (0.19 g).

Provenance & Evidence