HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl isocyanate → HCID 22243800, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | HCID 22386590 | HCID 22386590 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22243800 | HCID 22243800 | 64.3% |
Reaction Steps
4-Amino-5-(4-methoxyphenoxy)Quinazoline (1.0 g, 3.7 mmol) and phenyl isocyanate (0.52 g, 4.4 mmol) were reacted in 30 ml of dichloromethane according to procedure E to give 1-[5-(4-methoxyphenoxy)quinazolin-4-yl]-3-phenylurea (0.9 g, 64.3%, m.p. 231-232° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248771B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-9c2904f1db5f42a3866f076ebf9dbda2 |
| Source note | uspto-grants-2001_06 |