O-Methylhydroxylamine hydrochloride → HCID 178502653, compound

HRID 1067694Notes

Reaction equation

HRID 1067694 reaction equation
[NH:1]1[CH:5]=[C:4]([CH2:6][CH2:7][CH2:8][O:9][C:10]2[CH:15]=[CH:14][C:13]([C:16](=O)[CH3:17])=[CH:12][CH:11]=2)[N:3]=[CH:2]1.Cl.[CH3:20][O:21][NH2:22]>>[CH3:20][O:21][N:22]=[C:16]([C:13]1[CH:14]=[CH:15][C:10]([O:9][CH2:8][CH2:7][CH2:6][C:4]2[N:3]=[CH:2][NH:1][CH:5]=2)=[CH:11][CH:12]=1)[CH3:17]

Participants

3

Reactant 2

HCID 521874O-Methylhydroxylamine hydrochlorideHCID 178466793HCID 178466793, compound

Product 1

HCID 178502653HCID 178502653, compound

Procedure

1.2 mmol of (4-(3-(1H-imidazol-4-yl)propyloxy)phenyl)ethanone (Example 78) and 2.4 mmol of O-methylhydroxylamine hydrochloride are treated as described in Example 92.

Sources & evidence

ORD record
ord-190077a19f3948d094dce435882d9e75
Source dataset
uspto-grants-2001_06
Patent number
US06248765B1

Reaction notes

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