HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 178526338, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 178519714 | HCID 178519714 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178526338 | HCID 178526338 | — |
Reaction Steps
1.2 mmol of cyclopropyl 4-(3-(1H-imidazol-4-yl)propyloxy)phenyl ketone (Example 61) and 2.4 mmol of hydroxylamine hydrochloride in 20 ml of anhydrous ethanol are heated at 60° C. for 5 hours. The mixture is treated as described in Example 138, but isolated in the form of the free base.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248765B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-18e746d78d67495187d34c35748db1d0 |
| Source note | uspto-grants-2001_06 |