Ethyl Bromide → HCID 178467762, compound
Reaction equation
C1(C(C2C=CC=CC=2)(C2C=CC=CC=2)[N:8]2[CH:12]=[C:11]([CH2:13][CH2:14][CH2:15][OH:16])[N:10]=[CH:9]2)C=CC=CC=1.Br[CH2:30][CH3:31]>>[NH:8]1[CH:12]=[C:11]([CH2:13][CH2:14][CH2:15][O:16][CH2:30][CH3:31])[N:10]=[CH:9]1Participants
3
Procedure
5 mmol of 3-(1-triphenylmethyl-1H-imidazol-4-yl)propanol and 5 mmol of bromoethane are treated as described in Example 5. The title compound is crystallized in the form of hydrogen oxalate from ethanol and diethyl ether.
Workup
- customThe title compound is crystallized in the form of hydrogen oxalate from ethanol and diethyl ether
Sources & evidence
- ORD record
- ord-fc1762935807450a9ff9c158ccc42e2c
- Source dataset
- uspto-grants-2001_06
- Patent number
- US06248765B1
Reaction notes
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