HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 21194070, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 1-Hydroxy-1H-indole-2-carboxylic acid | HCID 21194199 | — |
| Product | HCID 21194070 | HCID 21194070 | 59.5% |
Reaction Steps
The reaction was carried out in a manner similar to Reference Example 6 except for using 3.99 g (22.5 mmol) of 1-hydroxy-2-indolecarboxylic acid, 5.36 g (45.0 mmol) of thionyl chloride and 100 ml of methanol. Thus 2.56 g (59.5%) of methyl 1-hydroxy-2-indolecarboxylate was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248772B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-16e47818614d4b14b93d6da71617f7e6 |
| Source note | uspto-grants-2001_06 |