HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → 1-[2-Oxo-2-(2-pyridyl)ethyl]pyridinium Iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | 2-Acetylpyridine | HCID 14286 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 1-[2-Oxo-2-(2-pyridyl)ethyl]pyridinium Iodide | HCID 213499 | — |
Reaction Steps
To a stirred solution of 2-acetylpyridine (0.5 mole) in 600 mL pyridine is added iodine (127 g; 0.5 mole). The mixture is heated on a steam bath for 45 minutes, and the product crystallizes on cooling. The solid is filtered and the crystalline cake is rinsed twice with methylene chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06248870B1 |
| Source dataset | uspto-grants-2001_06 |
| ORD ID | ord-c43e95c0a52643d99b7885d936a465ba |
| Source note | uspto-grants-2001_06 |